@InProceedings{AntunesLoboCoraTrav:2007:PrCaNa,
author = "Antunes, {\'E}rica Freire and Lobo, Anderson Oliveira and Corat,
Evaldo Jos{\'e} and Trava-Airoldi, Vladimir Jesus",
affiliation = "{Instituto Nacional de Pesquisas Espaciais (INPE)} and {Instituto
Nacional de Pesquisas Espaciais (INPE)} and {Instituto Nacional de
Pesquisas Espaciais (INPE)} and {Instituto Nacional de Pesquisas
Espaciais (INPE)}",
title = "Production of Carbon Nanotubes by Nebulized Spray Pyrolysis of the
Catalyst",
year = "2007",
organization = "Encontro sobre Diamante, Carbono Amorfo, Nanotubos de Carbono e
Materiais Relacionados.",
abstract = "The nebulized pyrolysis method is a technique similar to spray
pirolysis based on the simultaneous injection of a
metallocenehydrocarbon solution into the reaction furnace, using
an inert gas as carrier. The difference is the use of ultrasonic
methods to nebulize the solution, which allows forming smaller
particles. The major advantage of spray methods consists in the
direct and continuous generation of fresh catalytic particles
throughout the entire growth cycle. Our experiments are still in
lab scale, but there are possibilities to scale up the method for
continuous or semi-continuous production. In our case, we have
produced carbon nanotubes in a quartz tubular furnace with
diameter of 1 inch and length of 15cm, using a hexane solution of
ferrocene (20g/L), with argon or nitrogen as carrier gas at 200
sccm. The carbon nanotubes have grown in a thin film form,
aligned, on quartz wall, with thickness of 100-200 dm and diameter
between 50 and 100 nm during 10 min, revealed by scanning electron
microscopy. The Raman spectra show good crystalline quality. This
system produces ~0.1g of multiwalled carbon nanotubes at each
run.",
conference-location = "Fortaleza, CE",
conference-year = "24-26 out.",
language = "en",
urlaccessdate = "06 maio 2024"
}